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Isolation and Identification of β-Sitosterol and Stigmasterol Mixture from Root Bark of Slatri (Calophyllum soulattri Burm. f)


 
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1. Title Title of document Isolation and Identification of β-Sitosterol and Stigmasterol Mixture from Root Bark of Slatri (Calophyllum soulattri Burm. f)
 
2. Creator Author's name, affiliation, country Doni Eko Saputra; Jurusan Kimia, FMIPA, Universitas Sebelas Maret; Indonesia
 
2. Creator Author's name, affiliation, country Nestri Handayani; Jurusan Kimia, FMIPA, Universitas Sebelas Maret; Indonesia
 
2. Creator Author's name, affiliation, country Muhammad Widyo Wartono; Jurusan Kimia, FMIPA, Universitas Sebelas Maret; Indonesia
 
3. Subject Discipline(s) organic chemistry
 
3. Subject Keyword(s) Calophyllum soulattri; Root Barks; β-sitosterol; stigmasterol
 
4. Description Abstract

Chemical isolation and identificationof root bark of CalophyllumsoulattriBurm. f. have been conducted. Isolation was conducted by maceration with ethyl acetate as solvent. Ethyl acetate extract was separated and purified by vacuum liquid chromatography and flash chromatography which was guided by thin layer chromatography to obtain yellowish white solid. Isolated compounds were determined by spectroscopy methods such as UV, FTIR, 1H NMR, 13C NMR, DEPT, HSQC, HMBC and were compared to the references. Based on the analysis result it’s known that the compounds are the mixture of?-sitosterol and stigmasterol.

 
5. Publisher Organizing agency, location UNIVERSITAS SEBELAS MARET (UNS)
 
6. Contributor Sponsor(s)
 
7. Date (YYYY-MM-DD) 2018-05-24
 
8. Type Status & genre Peer-reviewed Article
 
8. Type Type
 
9. Format File format PDF
 
10. Identifier Uniform Resource Identifier https://jurnal.uns.ac.id/alchemy/article/view/14
 
10. Identifier Digital Object Identifier https://doi.org/10.20961/alchemy.10.1.14.87-93
 
11. Source Title; vol., no. (year) ALCHEMY Jurnal Penelitian Kimia; Vol 10, No 1 (2014): March
 
12. Language English=en en
 
13. Relation Supp. Files
 
14. Coverage Geo-spatial location, chronological period, research sample (gender, age, etc.)
 
15. Rights Copyright and permissions Copyright (c) 2016 ALCHEMY Jurnal Penelitian Kimia
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